ADVANCES IN COMPOSITE MATERIALS - ECODESIGN AND ANALYSIS
Experimental
1.3 Preparation of PVA-acid red mud nanocomposite materials and organically modified red mud nanocomposite materials
10% (w/v) aqueous solution of PVA was prepared by dissolving 10g of dried powdered PVA in 100ml of distilled water at a temperature of 100 oC with continuous stirring. Polymer modified red mud nanocomposite (PRM) films were made by mixing different loading percentage of acid modified red mud and organically modified red mud into the virgin PVA solution. The PVA-red mud solution thus obtained was sonicated for better dispersion and removal of any air bubble present in the solution. The solution was cast on the plane glass surface and dried at room temperature. The composition of the PRM materials was varied from 0 to 5 wt % of RM with respect to the PVA content.
1.4 Red mud loading levels
Sample index |
PVA |
SP1 |
SP2 |
SP3 |
SP4 |
SP5 |
SP6 |
SP7 |
% Loading of boric acid mod. red mud |
0 |
0.5 |
1.0 |
1.5 |
2.0 |
3.0 |
4.0 |
5.0 |
Sample index |
PVA |
CP1 |
CP2 |
CP3 |
CP4 |
CP5 |
CP6 |
CP7 |
% Loading of organically mod. red mud |
0 |
0.5 |
1.0 |
1.5 |
2.0 |
3.0 |
4.0 |
5.0 |
Sample index |
PVA |
PRM1 |
PRM2 |
PRM3 |
PRM4 |
PRM5 |
PRM6 |
PRM7 |
% Loading of Phosphomolybdic acid mod. red mud |
0 |
1.0 |
1.5 |
2.0 |
2.5 |
3.0 |
4.0 |
5.0 |
Table 2. Sample Designation |